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When the 1V-LSD hemitartrate salt was subjected to basification and extraction with diethyl ether ahead of GC-MS Investigation, it had been discovered that hydrolysis to LSD transpired (Supporting Data). Additionally, a few far more 1V-LSD isomers had been detected within the GC-MS TIC trace with 1V-LSD labeled as isomer I. When the 1V-LSD salt was